Static Headspace-Gas Chromatography  Theory and Practice, Second Edition Cover

Static Headspace-Gas Chromatography: Theory and Practice, Second Edition

ISBN/ASIN: 9780471749448,9780471914587 | 2006 | English | pdf | 366/366 pages | 2.59 Mb
Author: Bruno Kolb, Leslie S. Ettre(auth.)

The only reference to provide both current and thorough coverage of this important analytical technique

Static headspace-gas chromatography (HS-GC) is an indispensable technique for analyzing volatile organic compounds, enabling the analyst to assay a variety of sample matrices while avoiding the costly and time-consuming preparation involved with traditional GC.

Static Headspace-Gas Chromatography: Theory and Practice has long been the only reference to provide in-depth coverage of this method of analysis. The Second Edition has been thoroughly updated to reflect the most recent developments and practices, and also includes coverage of solid-phase microextraction (SPME) and the purge-and-trap technique. Chapters cover:
* Principles of static and dynamic headspace analysis, including the evolution of HS-GC methods and regulatory methods using static HS-GC
* Basic theory of headspace analysis-physicochemical relationships, sensitivity, and the principles of multiple headspace extraction
* HS-GC techniques-vials, cleaning, caps, sample volume, enrichment, and cryogenic techniques
* Sample handling
* Cryogenic HS-GC
* Method development in HS-GC
* Nonequilibrium static headspace analysis
* Determination of physicochemical functions such as vapor pressures, activity coefficients, and more

Comprehensive and focused, Static Headspace-Gas Chromatography, Second Edition provides an excellent resource to help the reader achieve optimal chromatographic results. Practical examples with original data help readers to master determinations in a wide variety of areas, such as forensic, environmental, pharmaceutical, and industrial applications.Content:
Chapter 1 General Introduction (pages 1–18):
Chapter 2 Theoretical Background of HS?GC and Its Applications (pages 19–50):
Chapter 3 The Technique of HS?GC (pages 51–163):
Chapter 4 Sample Handling in HS?GC (pages 165–196):
Chapter 5 Headspace Methods for Quantitative Analysis (pages 197–256):
Chapter 6 Method Development in HS?GC (pages 257–270):
Chapter 7 Nonequilibrium Static Headspace Analysis (pages 271–277):
Chapter 8 Qualitative Analysis by HS?GC (pages 279–291):
Chapter 9 Special Measurements (pages 293–333):

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